An Efficient Synthesis of 1,8-Dioxo-Octahydroxanthenes Derivatives Using Heterogeneous Ce-ZSM-11 Zeolite Catalyst

The Ce-ZSM-11 zeolite has been used as an efficient catalyst for the one pot synthesis of 1,8-dioxo-octahydroxanthene derivatives from aromatic aldehyde and 5,5-dimethyl-cyclohexane-1,3-dione under reflux condition. The catalyst was characterized by Powder X-ray diffraction (XRD), Scanning Electron...

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محفوظ في:
التفاصيل البيبلوغرافية
المؤلفون الرئيسيون: Magar, Rameshwar R. (مؤلف), Pawar, Ganesh T. (مؤلف), Gadekar, Sachin P. (مؤلف), Lande, Machhindra Karbhari (مؤلف)
مؤلفون آخرون: Department of Chemistry, Dr. Babasaheb Ambedkar Marathwada University, Aurangabad-431004 (MS) (مساهم)
التنسيق: EJournal Article
منشور في: Department of Chemical Engineering - Diponegoro University, 2018-12-04.
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الوصف
الملخص:The Ce-ZSM-11 zeolite has been used as an efficient catalyst for the one pot synthesis of 1,8-dioxo-octahydroxanthene derivatives from aromatic aldehyde and 5,5-dimethyl-cyclohexane-1,3-dione under reflux condition. The catalyst was characterized by Powder X-ray diffraction (XRD), Scanning Electron Microscopy (SEM), Energy Dispersive Spectroscopy (EDS), Fourier Transform Infrared Spectroscopy (FTIR), Brunauer-Emmer-Teller (BET) surface area analysis, and Temperature Programmed Desorption (TPD) techniques. This method provides several advantageous such as use of inexpensive catalyst, simple work-up procedure, high yield of desired product and reusability of catalyst. 
وصف المادة:https://ejournal2.undip.ac.id/index.php/bcrec/article/view/2062