Polymerization of Ethylene Glycol Dimethacrylate (EGDM), Using An Algerian Clay as Eco-catalyst (Maghnite-H+ and Maghnite-Na+)

In this paper we have explored a novel and green method to synthesis and polymerize ethylene glycol dimethacrylate (EGDM). This technique consists on using Maghnite (Algerian clay) as a green catalyst to replace toxic catalysts. The Algerian clay has been modified using two ion exchange process to o...

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Main Authors: Haoue, Sara (Author), Derdar, Hodhaifa (Author), Belbachir, Mohammed (Author), Harrane, Amine (Author)
Other Authors: Direction Générale de la Recherche Scientifique et du Développement Technologique-Algeria (Contributor)
Format: EJournal Article
Published: Department of Chemical Engineering - Diponegoro University, 2020-04-01.
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001 BCREC_UNDIP_6297_3636
042 |a dc 
100 1 0 |a Haoue, Sara  |e author 
100 1 0 |a Direction Générale de la Recherche Scientifique et du Développement Technologique-Algeria  |e contributor 
700 1 0 |a Derdar, Hodhaifa  |e author 
700 1 0 |a Belbachir, Mohammed  |e author 
700 1 0 |a Harrane, Amine  |e author 
245 0 0 |a Polymerization of Ethylene Glycol Dimethacrylate (EGDM), Using An Algerian Clay as Eco-catalyst (Maghnite-H+ and Maghnite-Na+) 
260 |b Department of Chemical Engineering - Diponegoro University,   |c 2020-04-01. 
500 |a https://ejournal2.undip.ac.id/index.php/bcrec/article/view/6297 
520 |a In this paper we have explored a novel and green method to synthesis and polymerize ethylene glycol dimethacrylate (EGDM). This technique consists on using Maghnite (Algerian clay) as a green catalyst to replace toxic catalysts. The Algerian clay has been modified using two ion exchange process to obtain Maghnite-H+ (proton exchanged process) and Maghnite-Na+ (sodium exchanged process). Synthesis experiments of EGDM and Poly (EGDM) are performed in bulk respecting the principles of green chemistry. The structure of the obtained monomer and the obtained polymer was confirmed by FT-IR, 1H-NMR and 13C-NMR, where the methacrylate end groups are clearly visible. The presence of unsaturated end group in the structure of monomer was confirmed by UV-Visible analysis. Thermogravimetric analysis (TGA) was used to study the thermal stability of these obtained products. Copyright © 2020 by Authors, Published by BCREC Group. This is an open access article under the CC BY-SA License (https://creativecommons.org/licenses/by-sa/4.0).  
540 |a Copyright (c) 2020 by Authors, Published by BCREC Group 
540 |a http://creativecommons.org/licenses/by-sa/4.0 
546 |a eng 
690 |a Ethylene glycol dimethacrylate; Green catalyst; Maghnite-H+; Maghnite-Na+; Anionic polymerization. 
655 7 |a info:eu-repo/semantics/article  |2 local 
655 7 |a info:eu-repo/semantics/publishedVersion  |2 local 
655 7 |2 local 
786 0 |n Bulletin of Chemical Reaction Engineering & Catalysis; 2020: BCREC Volume 15 Issue 1 Year 2020 (April 2020); 221-230 
786 0 |n 1978-2993 
787 0 |n https://ejournal2.undip.ac.id/index.php/bcrec/article/view/6297/3636 
787 0 |n https://ejournal2.undip.ac.id/index.php/bcrec/article/downloadSuppFile/6297/1603 
856 4 1 |u https://ejournal2.undip.ac.id/index.php/bcrec/article/view/6297/3636  |z Get Fulltext 
856 4 1 |u https://ejournal2.undip.ac.id/index.php/bcrec/article/downloadSuppFile/6297/1603  |z Get Fulltext