Modification, Characterization, and Catalytic Application of Mesolite for One Pot Synthesis of 3-Methyl-4-arylmethylene-isoxazol-5(4H)-ones
Natural mesolite type zeolite was collected, modified by sulphuric acid treatment and characterized by using Powder-X ray diffraction, Scanning electron microscopy and Energy dispersive spectroscopy, Fourier transform infrared spectroscopy. Temperature programmed ammonia desorption, Brunauer-Emmer-T...
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Department of Chemical Engineering - Diponegoro University,
2017-04-30.
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| LEADER | 02934 am a22003373u 4500 | ||
|---|---|---|---|
| 001 | BCREC_UNDIP_655_611 | ||
| 042 | |a dc | ||
| 100 | 1 | 0 | |a Pawar, Ganesh Trambakrao |e author |
| 100 | 1 | 0 | |a Department of Chemistry, Dr. Babasaheb Ambedkar Marathwada University Aurangabad-431004, Maharashtra |q (INDIA) |e contributor |
| 700 | 1 | 0 | |a Gadekar, Sachin Pandit |e author |
| 700 | 1 | 0 | |a Arbad, Balasaheb R. |e author |
| 700 | 1 | 0 | |a Lande, Machhindra Karbhari |e author |
| 245 | 0 | 0 | |a Modification, Characterization, and Catalytic Application of Mesolite for One Pot Synthesis of 3-Methyl-4-arylmethylene-isoxazol-5(4H)-ones |
| 260 | |b Department of Chemical Engineering - Diponegoro University, |c 2017-04-30. | ||
| 500 | |a https://ejournal2.undip.ac.id/index.php/bcrec/article/view/655 | ||
| 520 | |a Natural mesolite type zeolite was collected, modified by sulphuric acid treatment and characterized by using Powder-X ray diffraction, Scanning electron microscopy and Energy dispersive spectroscopy, Fourier transform infrared spectroscopy. Temperature programmed ammonia desorption, Brunauer-Emmer-Teller surface area analysis. Modified dealuminated mesolite shows an efficient catalytic activity for one pot synthesis of 3-methyl-4-arylmethylene-isoxazol-5(4H)-ones derivatives, via one pot three component condensation of benzaldehyde, ethylacetoacetate and hydroxylamine hydrochloride. Present method offers several advantages over the reported methods like a simple and inexpensive modification of catalyst, mild reaction condition, easy separation of catalyst, simple work-up procedure, nonchromatographic isolation and purification desired product and excellent yield. Furthermore, catalyst could be reused without significant loose in activity. | ||
| 540 | |a Copyright (c) 2017 by Authors, Published by BCREC Group | ||
| 540 | |a http://creativecommons.org/licenses/by-sa/4.0 | ||
| 546 | |a eng | ||
| 690 | |a 3-methyl-4-arylmethylene-isoxazol-5(4H)-ones; benzaldehyde; ethylacetoacetate; hyroxylaminehydrochloride; modification of mesolite; natural zeolite | ||
| 655 | 7 | |a info:eu-repo/semantics/article |2 local | |
| 655 | 7 | |a info:eu-repo/semantics/publishedVersion |2 local | |
| 655 | 7 | |2 local | |
| 786 | 0 | |n Bulletin of Chemical Reaction Engineering & Catalysis; 2017: BCREC Volume 12 Issue 1 Year 2017 (April 2017); 32-40 | |
| 786 | 0 | |n 1978-2993 | |
| 787 | 0 | |n https://ejournal2.undip.ac.id/index.php/bcrec/article/view/655/611 | |
| 787 | 0 | |n https://ejournal2.undip.ac.id/index.php/bcrec/article/downloadSuppFile/655/70 | |
| 787 | 0 | |n https://ejournal2.undip.ac.id/index.php/bcrec/article/downloadSuppFile/655/71 | |
| 856 | 4 | 1 | |u https://ejournal2.undip.ac.id/index.php/bcrec/article/view/655/611 |z Get Fulltext |
| 856 | 4 | 1 | |u https://ejournal2.undip.ac.id/index.php/bcrec/article/downloadSuppFile/655/70 |z Get Fulltext |
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