Synergistic Effect of Microwave Calcination and Sonophotocatalytic Activity of TiO2-Montmorillonite on The Degradation of Direct Yellow 106 and Disperse Violet 1

The TiO2-pillared montmorillonite nanoparticles (TiO2-Mt) were prepared by the sol-gel method, then applied for the elimination of dyes in solution: CI Direct Yellow 106 (DY106) (azo dye) and CI Disperse Violet 1 (DV1) (anthraquinone dye) by the sonocatalytic, photocatalytic and sonophotocatalytic p...

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Main Authors: Labib, Issma (Author), Boutoumi, Hocine (Author), Khalaf, Hussein (Author)
Other Authors: Direction Générale de la Recherche Scientifique et du Développement Technologique (DGRSDT) (Contributor)
Format: EJournal Article
Published: Department of Chemical Engineering - Diponegoro University, 2020-08-01.
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042 |a dc 
100 1 0 |a Labib, Issma  |e author 
100 1 0 |a Direction Générale de la Recherche Scientifique et du Développement Technologique   |q  (DGRSDT)   |e contributor 
700 1 0 |a Boutoumi, Hocine  |e author 
700 1 0 |a Khalaf, Hussein  |e author 
245 0 0 |a Synergistic Effect of Microwave Calcination and Sonophotocatalytic Activity of TiO2-Montmorillonite on The Degradation of Direct Yellow 106 and Disperse Violet 1 
260 |b Department of Chemical Engineering - Diponegoro University,   |c 2020-08-01. 
500 |a https://ejournal2.undip.ac.id/index.php/bcrec/article/view/6999 
520 |a The TiO2-pillared montmorillonite nanoparticles (TiO2-Mt) were prepared by the sol-gel method, then applied for the elimination of dyes in solution: CI Direct Yellow 106 (DY106) (azo dye) and CI Disperse Violet 1 (DV1) (anthraquinone dye) by the sonocatalytic, photocatalytic and sonophotocatalytic processes, in order to test the efficiency of photocatalysts, while photolysis, sonolysis, and sonophotolysis tests have been done previously. The photocatalysts (TiO2-Mt) were characterized by X-ray Diffraction (XRD), X-ray Fluorescence analysis (XRF), Brunauer-Emmet-Teller (BET), Scanning Electron Microscopy (SEM) methods, thermal and thermogravimetric analysis (TG/DTA) and the zero load point (pHpzc). Aqueous solutions of dye of an initial concentration (50 mg/L), in the presence of 1 g/L of photocatalyst, were irradiated using a mercury lamp (Hg) of 40 Mw/cm2 and put in contact with an ultrasonic probe with a frequency of 20 kHz and a power of 750 W, providing the ultrasound. The results obtained indicate that a weak, good and better dye degradation rate has been observed successively by the application of the sonocatalytic, photocatalytic and sonophotocatalytic processes, where the latter has shown a synergistic effect, while the photocatalyst TiO2-Mt/MW showed significant efficiency during the degradation, due to the beneficial effect of the microwave calcination mode. Copyright © 2020 by Authors, Published by BCREC Group. This is an open access article under the CC BY-SA License (https://creativecommons.org/licenses/by-sa/4.0).  
540 |a Copyright (c) 2020 by Authors, Published by BCREC Group 
540 |a http://creativecommons.org/licenses/by-sa/4.0 
546 |a eng 
690 |a TiO2-Montmorillonite; microwave calcinations; Sonophotocatalysis; Direct Yellow 106; Disperse Violet 1 
655 7 |a info:eu-repo/semantics/article  |2 local 
655 7 |a info:eu-repo/semantics/publishedVersion  |2 local 
655 7 |2 local 
786 0 |n Bulletin of Chemical Reaction Engineering & Catalysis; 2020: BCREC Volume 15 Issue 2 Year 2020 (August 2020); 304-318 
786 0 |n 1978-2993 
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