Synthesis of SrO.SiO2 Catalyst and Its Application in the Transesterification Reactions of Soybean Oil

The synthesis and characterization of SrO.SiO2 were carried out. The rice hull ash was utilized as a source for SiO2. The SrO.SiO2 was prepared by sol-gel technique, and the ratios of SrO:SiO2 were      varied as 0:1, 1:0, 3:2, 2:4, and 2:7. The sol-gel was calcined at 800 oC for 4 hours. The result...

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Main Authors: Widiarti, Nuni (Author), Suryana, Lisa Amalia (Author), Wijayati, Nanik (Author), Rahayu, Endah Fitriani (Author), Harjito, Harjito (Author), Wardhana, Samuel Budi (Author), Prasetyoko, Didik (Author), Suprapto, Suprapto (Author)
Format: EJournal Article
Published: Department of Chemical Engineering - Diponegoro University, 2017-08-01.
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001 BCREC_UNDIP_804_918
042 |a dc 
100 1 0 |a Widiarti, Nuni  |e author 
100 1 0 |e contributor 
700 1 0 |a Suryana, Lisa Amalia  |e author 
700 1 0 |a Wijayati, Nanik  |e author 
700 1 0 |a Rahayu, Endah Fitriani  |e author 
700 1 0 |a Harjito, Harjito  |e author 
700 1 0 |a Wardhana, Samuel Budi  |e author 
700 1 0 |a Prasetyoko, Didik  |e author 
700 1 0 |a Suprapto, Suprapto  |e author 
245 0 0 |a Synthesis of SrO.SiO2 Catalyst and Its Application in the Transesterification Reactions of Soybean Oil 
260 |b Department of Chemical Engineering - Diponegoro University,   |c 2017-08-01. 
500 |a https://ejournal2.undip.ac.id/index.php/bcrec/article/view/804 
520 |a The synthesis and characterization of SrO.SiO2 were carried out. The rice hull ash was utilized as a source for SiO2. The SrO.SiO2 was prepared by sol-gel technique, and the ratios of SrO:SiO2 were      varied as 0:1, 1:0, 3:2, 2:4, and 2:7. The sol-gel was calcined at 800 oC for 4 hours. The result was    characterized using XRD and FTIR. The diffraction pattern shows that the diffraction angle was shifted, and the intensity of the main peaks was increased. This research indicated that the            crystallinity of SrO was improved at the higher SiO content. Further, a new peak was observed in the IR spectra at a wavenumber of 900 cm-1 indicating the appearance of new functional groups of the SrO.SiO2. The catalytic activity of SrO.SiO2 on transesterification reaction was optimized. The optimum condition was obtained at SrO.SiO2 of 2:7, reaction time of 30 minutes, reaction temperature of 65 oC, the amount of catalyst of 1 % w/v of reactants, and the biodiesel yield of 96.66 %.  
540 |a Copyright (c) 2017 by Authors, Published by BCREC Group 
540 |a http://creativecommons.org/licenses/by-sa/4.0 
546 |a eng 
690 |a biodiesel, catalyst, SrO/SiO2, soybean oil, transesterification 
655 7 |a info:eu-repo/semantics/article  |2 local 
655 7 |a info:eu-repo/semantics/publishedVersion  |2 local 
655 7 |2 local 
786 0 |n Bulletin of Chemical Reaction Engineering & Catalysis; 2017: BCREC Volume 12 Issue 2 Year 2017 (August 2017); 299-305 
786 0 |n 1978-2993 
787 0 |n https://ejournal2.undip.ac.id/index.php/bcrec/article/view/804/918 
787 0 |n https://ejournal2.undip.ac.id/index.php/bcrec/article/downloadSuppFile/804/115 
856 4 1 |u https://ejournal2.undip.ac.id/index.php/bcrec/article/view/804/918  |z Get Fulltext 
856 4 1 |u https://ejournal2.undip.ac.id/index.php/bcrec/article/downloadSuppFile/804/115  |z Get Fulltext